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Vertically Aligned FeOOH/NiFe Layered Double Hydroxides Electrode for Highly Efficient Oxygen Evolution Reaction

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Fuel Cell System and Engineering Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, 116023, P. R. China
University of Chinese Academy of Sciences, Beijing, 100049, P. R. China
*E-mail: [email protected] (H.Y.).
*E-mail: [email protected] (Z.S.).
Cite this: ACS Appl. Mater. Interfaces 2017, 9, 1, 464–471
Publication Date (Web):December 14, 2016
https://doi.org/10.1021/acsami.6b13360
Copyright © 2016 American Chemical Society
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Abstract

Employing a low-cost and highly efficient electrocatalyst to replace Ir-based catalysts for oxygen evolution reaction (OER) has drawn increasing interest in renewable energy storage. In this work, a vertically aligned FeOOH/NiFe layered double hydroxides (LDHs) nanosheets supported on Ni foam (VA FeOOH/NiFe LDHs-NF) is prepared as a highly effective OER electrode in alkaline electrolyte. The VA FeOOH/NiFe LDHs-NF represents nanosheet arrays on nickel foam with some interspace among them. The vertically aligned and interlayer-structured architecture is binder-free and contributes to facile strain relaxation, relieving the exfoliation of the catalysts layer caused by the oxygen evolution process. The as-prepared electrode shows current densities of 10 and 500 mA cm–2 at overpotentials of 208 and 288 mV, and good stability in a half-cell electrolyzer. Besides, the alkaline polymer electrolyte water electrolyzer (APEWE) with this electrode showed 1.71 V at 200 mA cm–2, and 2.041 V at 500 mA cm–2, exhibiting the corresponding energy efficiency of 86.0% and 72.0% (based on the lower heating value of hydrogen), which is better than the typical commercial alkaline water electrolyzer.

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  • Images of XRD patterns of as-prepared samples with different mole ratio images and XPS spectrum of VA FeOOH/NiFe LDHs-NF as well as calibration of reference electrode (Figures S1–S3); iV curves of VA FeOOH/NiFe LDHs-NF, Fe LDHs-NF, bare NF, and Ir black without iR-correction (Figure S4); Tafel plots of VA FeOOH/NiFe LDHs-NF, Fe LDHs-NF for OER (Figure S5); Nyquist plots and Bode plots of VA FeOOH/NiFe LDHs-NF, Ni LDHs-NF, and Fe LDHs-NF (Figures S6–S9); cyclic voltammograms in the double-layer region of VA FeOOH/NiFe LDHs-NF, Ni LDHs-NF, and Fe LDHs-NF recorded at different scan rates (Figures S10–S12); cyclic voltammogram curves of VA FeOOH/NiFe LDHs-NF, Ni LDHs-NF, and Fe LDHs-NF (Figure S13); summary of results for representative nonprecious-metal OER electrocatalysts reported in the literatures (Table S1); summary of fitted EIS data for VA FeOOH/NiFe LDHs-NF, Ni LDHs-NF, and Fe LDHs-NF (Table S2) (PDF)

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